4CY9
DpsA14 from Streptomyces coelicolor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | F 41 3 2 |
| Unit cell lengths | 209.660, 209.660, 209.660 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 121.050 - 1.780 |
| R-factor | 0.15351 |
| Rwork | 0.153 |
| R-free | 0.17088 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.035 |
| RMSD bond angle | 2.825 |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 48.100 |
| High resolution limit [Å] | 1.780 |
| Rmerge | 0.090 |
| Number of reflections | 38297 |
| <I/σ(I)> | 19.4 |
| Completeness [%] | 99.9 |
| Redundancy | 11.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 0.2 M NACL, 0.1 M SODIUM CACODYLATE PH 6.5, 0.2 M AMMONIUM SULPHATE |
