4CWS
Human HSP90 alpha N-terminal domain in complex with an Aminotriazoloquinazoline inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-04-15 |
Detector | MAR scanner 345 mm plate |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 67.143, 91.529, 99.432 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.300 |
R-factor | 0.20602 |
Rwork | 0.203 |
R-free | 0.26394 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.013 |
RMSD bond angle | 1.741 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.050 | 0.270 |
Number of reflections | 12942 | |
<I/σ(I)> | 17.1 | 5.8 |
Completeness [%] | 93.6 | 95.5 |
Redundancy | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |