4CWF
Human HSP90 alpha N-terminal domain in complex with an Aminotriazoloquinazoline inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-05-24 |
Detector | MAR scanner 345 mm plate |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 66.502, 90.325, 98.018 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 66.370 - 2.000 |
R-factor | 0.20171 |
Rwork | 0.200 |
R-free | 0.23337 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.435 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.080 | 0.270 |
Number of reflections | 23787 | |
<I/σ(I)> | 13.8 | 4.3 |
Completeness [%] | 96.9 | 85.8 |
Redundancy | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |