4CVT
Structure of Apobacterioferritin Y58F variant
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-11-05 |
| Detector | ADSC CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 104.460, 28.070, 56.810 |
| Unit cell angles | 90.00, 119.18, 90.00 |
Refinement procedure
| Resolution | 46.817 - 1.794 |
| R-factor | 0.169 |
| Rwork | 0.167 |
| R-free | 0.21420 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2vxi |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.814 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.820 | 1.840 |
| High resolution limit [Å] | 1.410 | 1.790 |
| Rmerge | 0.090 | 0.580 |
| Number of reflections | 13671 | |
| <I/σ(I)> | 7.39 | 1.31 |
| Completeness [%] | 99.0 | 98.6 |
| Redundancy | 3.11 | 3.03 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
