4CVL
PaMurF in complex with AMP-PNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.580, 87.380, 91.520 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 63.200 - 2.980 |
R-factor | 0.21766 |
Rwork | 0.214 |
R-free | 0.29498 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.525 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 63.200 | 3.060 |
High resolution limit [Å] | 2.980 | 2.980 |
Rmerge | 0.190 | 1.020 |
Number of reflections | 10089 | |
<I/σ(I)> | 12.9 | 3.9 |
Completeness [%] | 99.9 | 99.7 |
Redundancy | 12.7 | 13.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.2 M CACL2, 0.1M TRIS (PH 8.5), 20 % PEG 6K |