4CV4
PIH N-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-03-01 |
Detector | SATURN |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 69.860, 50.140, 35.180 |
Unit cell angles | 90.00, 103.21, 90.00 |
Refinement procedure
Resolution | 34.249 - 1.902 |
R-factor | 0.1207 |
Rwork | 0.119 |
R-free | 0.15850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ckt |
RMSD bond length | 0.015 |
RMSD bond angle | 1.255 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.250 | 2.160 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.080 | 0.170 |
Number of reflections | 8928 | |
<I/σ(I)> | 22.7 | 14.9 |
Completeness [%] | 98.1 | 96.4 |
Redundancy | 4.3 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 0.02M MAGNESIUM CHLORIDE HEXAHYDRATE, 0.002M COBALT (2) CHLORIDE, 0.05M HEPES PH 7.5, 2M AMMONIUM SULFATE, 0.001M SPERMINE |