4CUU
Crystal structure of human BAZ2B in complex with fragment-6 N09645
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-03-10 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 81.451, 96.521, 57.968 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.544 - 1.801 |
R-factor | 0.1687 |
Rwork | 0.167 |
R-free | 0.20830 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.109 |
Data reduction software | XDS |
Data scaling software | Aimless |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.980 | 1.840 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.080 | 0.680 |
Number of reflections | 21028 | |
<I/σ(I)> | 14.7 | 2.1 |
Completeness [%] | 97.7 | 82.9 |
Redundancy | 6.5 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 30% PEG600, 0.1M MES PH 6.0 |