4CUS
Crystal structure of human BAZ2B in complex with fragment-4 N09496
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-03-10 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 82.175, 96.928, 57.978 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.656 - 1.783 |
| R-factor | 0.1681 |
| Rwork | 0.167 |
| R-free | 0.20270 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.085 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.070 | 1.820 |
| High resolution limit [Å] | 1.780 | 1.780 |
| Rmerge | 0.060 | 0.810 |
| Number of reflections | 22220 | |
| <I/σ(I)> | 17.1 | 1.8 |
| Completeness [%] | 98.9 | 82.5 |
| Redundancy | 6.5 | 5.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6 | 30% PEG600, 0.1M MES PH 6.0 |
