4CUQ
Crystal structure of human BAZ2B in complex with fragment-2 N09594
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-04-30 |
Detector | DECTRIS PIXEL |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 82.760, 96.500, 57.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 17.866 - 2.110 |
R-factor | 0.1699 |
Rwork | 0.167 |
R-free | 0.22570 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.992 |
Data scaling software | Aimless |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.850 | 2.160 |
High resolution limit [Å] | 2.110 | 2.110 |
Rmerge | 0.060 | 0.730 |
Number of reflections | 13598 | |
<I/σ(I)> | 18.2 | 2.8 |
Completeness [%] | 99.5 | 99.2 |
Redundancy | 5.5 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.4 | 33% PEG SMEAR LOW, 0.1M MES PH 6.4 |