4CUP
Crystal structure of human BAZ2B in complex with fragment-1 N09421
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-04-29 |
| Detector | DECTRIS PILATUS |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 80.370, 96.120, 57.670 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 18.538 - 1.880 |
| R-factor | 0.1779 |
| Rwork | 0.176 |
| R-free | 0.20780 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.898 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 32.970 | 1.930 |
| High resolution limit [Å] | 1.880 | 1.880 |
| Rmerge | 0.060 | 0.740 |
| Number of reflections | 18470 | |
| <I/σ(I)> | 16.2 | 1.9 |
| Completeness [%] | 99.5 | 98.6 |
| Redundancy | 5.4 | 4.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.4 | 34% PEG SMEAR LOW, 0.1M MES PH 6.4 |
