4CT5
DDX6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-07-05 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 113.116, 113.144, 77.183 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.590 - 3.000 |
R-factor | 0.2329 |
Rwork | 0.231 |
R-free | 0.26240 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wax |
RMSD bond length | 0.004 |
RMSD bond angle | 0.788 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.000 | 3.170 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.080 | 0.660 |
Number of reflections | 27769 | |
<I/σ(I)> | 11.7 | 2.4 |
Completeness [%] | 99.4 | 98.8 |
Redundancy | 5.2 | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 17% (W/V) PEG 10000, 100 MM BIS-TRIS PH 5.5 AND 100 MM AMMONIUM ACETATE |