4CSO
The structure of OrfY from Thermoproteus tenax
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 97.318, 101.472, 170.784 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.988 - 2.600 |
R-factor | 0.1907 |
Rwork | 0.188 |
R-free | 0.23570 |
Structure solution method | MIRAS |
Starting model (for MR) | NONE |
RMSD bond length | 0.015 |
RMSD bond angle | 1.460 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHARP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.980 | 2.750 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.120 | 1.100 |
Number of reflections | 26330 | |
<I/σ(I)> | 11.03 | 1.55 |
Completeness [%] | 99.4 | 96.7 |
Redundancy | 4.1 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | pH 6.5 |