4CSG
Structural insights into Toscana virus RNA encapsidation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-02-22 |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | P 65 |
Unit cell lengths | 104.484, 104.484, 510.763 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.124 - 3.320 |
R-factor | 0.241 |
Rwork | 0.240 |
R-free | 0.26780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | HOMOLOGY MODEL BASED ON 3OUO |
RMSD bond length | 0.003 |
RMSD bond angle | 0.713 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 3.410 |
High resolution limit [Å] | 3.320 | 3.320 |
Rmerge | 0.010 | 0.510 |
Number of reflections | 45886 | |
<I/σ(I)> | 10.7 | 2.4 |
Completeness [%] | 99.1 | 94.5 |
Redundancy | 4.2 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5 | 6.5% PEG 3350, 0.1 M SODIUM MALONATE, PH 4.5-5.2 |