4CSE
PIH N-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-02-05 |
Detector | DECTRIS PILATUS 2M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.220, 67.730, 104.020 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.759 - 3.300 |
R-factor | 0.2176 |
Rwork | 0.213 |
R-free | 0.30550 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ckt |
RMSD bond length | 0.010 |
RMSD bond angle | 1.298 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.760 | 3.480 |
High resolution limit [Å] | 3.300 | 3.300 |
Rmerge | 0.170 | 0.600 |
Number of reflections | 5693 | |
<I/σ(I)> | 12.8 | 4.7 |
Completeness [%] | 99.6 | 99.8 |
Redundancy | 11.7 | 12.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 0.15M SODIUM POTASSIUM PHOSPHATE, 20% PEG 3350, 0.1M BIS-TRIS PH 6.5 |