4CQX
H5 (tyTy) Del133/Ile155Thr Mutant Haemagglutinin in Complex with Human Receptor Analogue 6'SLN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 87.824, 117.104, 101.275 |
Unit cell angles | 90.00, 92.58, 90.00 |
Refinement procedure
Resolution | 101.170 - 2.300 |
R-factor | 0.1877 |
Rwork | 0.186 |
R-free | 0.22612 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4bgz |
RMSD bond length | 0.007 |
RMSD bond angle | 1.238 |
Data reduction software | xia2 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0046) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 87.730 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.090 | 0.650 |
Number of reflections | 90479 | |
<I/σ(I)> | 9.9 | 2 |
Completeness [%] | 99.6 | 100 |
Redundancy | 3.4 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BIS-TRIS PROPANE PH 7.5, 0.05 - 0.15 M K/NAPO4 (PH 7.0), 15-18% PEG 3350 |