4CPP
CRYSTAL STRUCTURES OF CYTOCHROME P450-CAM COMPLEXED WITH CAMPHANE, THIOCAMPHOR, AND ADAMANTANE: FACTORS CONTROLLING P450 SUBSTRATE HYDROXYLATION
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 108.670, 103.900, 36.380 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 2.110 |
R-factor | 0.184 |
RMSD bond length | 0.019 |
RMSD bond angle | 0.037 * |
Refinement software | PROFFT |
Data quality characteristics
Overall | |
Rmerge | 0.079 * |
Total number of observations | 144737 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | P-450CAM | 1 (mM) | camphor free |
2 | 1 | 1 | 250 (mM) | ||
3 | 1 | 1 | dithiothreitol | 50 (mM) | |
4 | 1 | 2 | ammonium sulfate | 66-70 (%sat) | with 5M KOH |