4COZ
Crystal Structure of Epithelial Adhesin 6 A domain (Epa6A) from Candida glabrata in complex with Galb1-3GlcNAc
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-10-20 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.280, 61.260, 106.620 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 53.170 - 2.300 |
R-factor | 0.17994 |
Rwork | 0.178 |
R-free | 0.22029 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PRUNED VERSION OF PDB ENTRY 4AF9 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.265 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.120 | 2.370 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmerge | 0.170 | 0.650 |
Number of reflections | 13420 | |
<I/σ(I)> | 12.1 | 3.5 |
Completeness [%] | 99.9 | 100 |
Redundancy | 9 | 9.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.08 M SODIUM ACETATE PH4.6, 1.6 M AMMONIUM SULFATE, 20% GLYCEROL, 0.05 M LACTOSE, 291 K, VAPOR DIFFUSION IN SITTING DROP, SOAKED WITH GALB1-3GLCNAC |