4COV
Crystal Structure of Epithelial Adhesin 6 A domain (Epa6A) from Candida glabrata in complex with Gala1-3Gal
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-02-14 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.520, 63.290, 110.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.580 - 1.500 |
R-factor | 0.15034 |
Rwork | 0.150 |
R-free | 0.17661 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PRUNED VERSION OF PDB ENTRY 4AF9 |
RMSD bond length | 0.005 |
RMSD bond angle | 1.201 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.580 | 1.580 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.050 | 0.520 |
Number of reflections | 47367 | |
<I/σ(I)> | 20.7 | 3 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 5.4 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.01 M SODIUM ACETATE PH 4.6, 30% PEG4000, 0.2 M AMMONIUM ACETATE, 0.05 M LACTOSE, 291 K, VAPOR DIFFUSION IN SITTING DROP, SOAKED WITH GALA1-3GAL |