4CKT
PIH1 N-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-09-30 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.020, 62.150, 114.290 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.599 - 3.000 |
R-factor | 0.2267 |
Rwork | 0.224 |
R-free | 0.28140 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.011 |
RMSD bond angle | 1.838 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | SHELX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 61.670 | 3.140 |
High resolution limit [Å] | 3.060 | 3.060 |
Rmerge | 0.120 | 0.520 |
Number of reflections | 68364 | |
<I/σ(I)> | 15.4 | 2.5 |
Completeness [%] | 90.1 | 56.4 |
Redundancy | 10.8 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | pH 7 |