4CJ0
Crystal structure of CelD in complex with affitin E12
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Spacegroup name | P 43 |
Unit cell lengths | 87.633, 87.633, 97.426 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.850 - 1.100 |
R-factor | 0.10773 |
Rwork | 0.107 |
R-free | 0.12546 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1clc |
RMSD bond length | 0.026 |
RMSD bond angle | 2.030 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.710 | 1.120 |
High resolution limit [Å] | 1.100 | 1.100 |
Rmerge | 0.110 | 0.750 |
Number of reflections | 292047 | |
<I/σ(I)> | 10.5 | 2.9 |
Completeness [%] | 98.4 | 96.3 |
Redundancy | 5.8 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |