4CIK
plasminogen kringle 1 in complex with inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | RIGAKU CCD |
| Spacegroup name | I 21 21 21 |
| Unit cell lengths | 50.777, 57.594, 81.414 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.040 - 1.780 |
| R-factor | 0.2529 |
| Rwork | 0.251 |
| R-free | 0.29220 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1ceb |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | BUSTER-TNT (2.5.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.800 | 1.830 |
| High resolution limit [Å] | 1.780 | 1.780 |
| Rmerge | 0.070 | 0.140 |
| Number of reflections | 11799 | |
| <I/σ(I)> | 22.6 | 10.2 |
| Completeness [%] | 100.0 | 99.9 |
| Redundancy | 6.8 | 6.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
