4CIK
plasminogen kringle 1 in complex with inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | RIGAKU CCD |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 50.777, 57.594, 81.414 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.040 - 1.780 |
R-factor | 0.2529 |
Rwork | 0.251 |
R-free | 0.29220 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ceb |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | BUSTER-TNT (2.5.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.800 | 1.830 |
High resolution limit [Å] | 1.780 | 1.780 |
Rmerge | 0.070 | 0.140 |
Number of reflections | 11799 | |
<I/σ(I)> | 22.6 | 10.2 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 6.8 | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |