4CGE
Crystal structure of Mycobacterium tuberculosis Resuscitation promoting factor E
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.3.1 |
| Synchrotron site | ALS |
| Beamline | 8.3.1 |
| Temperature [K] | 100 |
| Collection date | 2012-07-13 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 34.543, 84.004, 72.628 |
| Unit cell angles | 90.00, 103.53, 90.00 |
Refinement procedure
| Resolution | 42.002 - 2.756 |
| R-factor | 0.2364 |
| Rwork | 0.234 |
| R-free | 0.28990 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.580 |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 42.000 |
| High resolution limit [Å] | 2.760 |
| Rmerge | 0.130 |
| Number of reflections | 10498 |
| Completeness [%] | 94.5 |
| Redundancy | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
