4CFP

Crystal structure of MltC in complex with tetrasaccharide at 2.15 A resolution

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Spacegroup name	P 1 21 1
Unit cell lengths	49.510, 114.330, 61.771
Unit cell angles	90.00, 93.28, 90.00

Refinement procedure

Resolution	49.429 - 2.150
R-factor	0.1951
Rwork	0.191
R-free	0.26780
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	NONE
RMSD bond length	0.008
RMSD bond angle	1.174
Phasing software	MOLREP
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.430	2.330
High resolution limit [Å]	2.150	2.150
Rmerge	0.110
Number of reflections	37159
<I/σ(I)>	6.6	1.9
Completeness [%]	99.7	99.8
Redundancy	5.4	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1