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4CFH

Structure of an active form of mammalian AMPK

Replaces:  2Y94
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I03
Synchrotron siteDiamond
BeamlineI03
Temperature [K]100
Detector technologyCCD
Collection date2009-07-06
DetectorADSC CCD
Spacegroup nameP 41 21 2
Unit cell lengths133.917, 133.917, 141.896
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution29.530 - 3.240
R-factor0.2343
Rwork0.233
R-free0.26770
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)PDB ENTRIES 2V8Q AND 2H6D
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwarePHENIX
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]29.5303.440
High resolution limit [Å]3.2403.240
Rmerge0.0700.510
Number of reflections18662
<I/σ(I)>122
Completeness [%]93.395.8
Redundancy4.54.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP291CRYSTALS WERE GROWN BY THE HANGING DROP METHOD WITH RESERVOIR SOLUTION CONTAINING 8% ISOPROPANOL AND 5% MPD AS PRECIPITANT IN 0.1M TRIS AT PH 7.5 AT 18 DEGREES.

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건을2024-09-18부터공개중

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