4CDJ
Structure of ZNRF3 ectodomain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 35.686, 73.503, 58.573 |
| Unit cell angles | 90.00, 97.49, 90.00 |
Refinement procedure
| Resolution | 45.567 - 1.500 |
| R-factor | 0.1625 |
| Rwork | 0.162 |
| R-free | 0.17730 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.842 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 45.570 |
| High resolution limit [Å] | 1.500 |
| Rmerge | 0.020 |
| Number of reflections | 46197 |
| <I/σ(I)> | 24.1 |
| Completeness [%] | 96.6 |
| Redundancy | 2.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 0.2 M AMMONIUM FORMATE AT PH 6.6 WITH 20% W/V PEG3350 |
