4CD1

RnNTPDase2 in complex with PSB-071

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	BESSY BEAMLINE 14.2
Synchrotron site	BESSY
Beamline	14.2
Temperature [K]	100
Detector technology	CCD
Collection date	2009-04-01
Detector	MARMOSAIC 225 mm CCD
Spacegroup name	P 21 21 21
Unit cell lengths	41.007, 68.040, 162.389
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.630 - 2.000
R-factor	0.19556
Rwork	0.193
R-free	0.23854
Structure solution method	OTHER
RMSD bond length	0.019
RMSD bond angle	2.093
Refinement software	REFMAC (5.7.0029)

Data quality characteristics

	Overall
Low resolution limit [Å]	36.600
High resolution limit [Å]	2.000
Rmerge	0.060
Number of reflections	30632
<I/σ(I)>	13.8
Completeness [%]	96.8
Redundancy	4.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1