4CD1
RnNTPDase2 in complex with PSB-071
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.2 |
| Synchrotron site | BESSY |
| Beamline | 14.2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-04-01 |
| Detector | MARMOSAIC 225 mm CCD |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 41.007, 68.040, 162.389 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 36.630 - 2.000 |
| R-factor | 0.19556 |
| Rwork | 0.193 |
| R-free | 0.23854 |
| Structure solution method | OTHER |
| RMSD bond length | 0.019 |
| RMSD bond angle | 2.093 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 36.600 |
| High resolution limit [Å] | 2.000 |
| Rmerge | 0.060 |
| Number of reflections | 30632 |
| <I/σ(I)> | 13.8 |
| Completeness [%] | 96.8 |
| Redundancy | 4.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
