4CBZ

Notch ligand, Jagged-1, contains an N-terminal C2 domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID29
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	100
Detector technology	PIXEL
Collection date	2012-06-08
Detector	DECTRIS PILATUS 6M
Spacegroup name	P 1
Unit cell lengths	56.930, 59.840, 62.940
Unit cell angles	95.04, 101.90, 98.70

Refinement procedure

Resolution	61.120 - 2.500
R-factor	0.2065
Rwork	0.204
R-free	0.24590
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2vj2
RMSD bond length	0.008
RMSD bond angle	1.120
Refinement software	BUSTER (2.11.4)

Data quality characteristics

	Overall
Low resolution limit [Å]	61.120
High resolution limit [Å]	2.500
Rmerge	0.120
Number of reflections	22857
Completeness [%]	82.8
Redundancy	3.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1