4CBA
Structural of delta 1-76 CTNNBL1 in space group I222
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-05-19 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 87.422, 92.848, 194.949 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.920 - 3.100 |
R-factor | 0.21953 |
Rwork | 0.216 |
R-free | 0.27846 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4cb8 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.744 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.300 | 3.300 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.100 | 0.400 |
Number of reflections | 14575 | |
<I/σ(I)> | 10.5 | 3.6 |
Completeness [%] | 98.8 | 98.4 |
Redundancy | 5 | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.12M ETHYLENE GLYCOL, 12.5% PEG 3350, 12.5% PEG 1K, 12.5% MPD, 0.1 M BICINE/TRIZMA BASE |