4CB9
Structure of full-length CTNNBL1 in P43212 space group
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-05-19 |
| Detector | ADSC CCD |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 66.727, 66.727, 325.883 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 65.460 - 3.000 |
| R-factor | 0.22216 |
| Rwork | 0.218 |
| R-free | 0.29867 |
| Structure solution method | MAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.351 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 81.470 | 3.200 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.110 | 0.920 |
| Number of reflections | 15841 | |
| <I/σ(I)> | 16.4 | 3.1 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 13.4 | 13.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8.5 | 0.1M TRIS PH 8.5, 1.1M NAF |
