4C9B
Crystal structure of eIF4AIII-CWC22 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-05-02 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 56.290, 108.720, 61.370 |
Unit cell angles | 90.00, 99.94, 90.00 |
Refinement procedure
Resolution | 55.445 - 2.000 |
R-factor | 0.2035 |
Rwork | 0.202 |
R-free | 0.23580 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.006 |
RMSD bond angle | 0.872 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.400 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.090 | 0.640 |
Number of reflections | 48938 | |
<I/σ(I)> | 12.68 | 2.17 |
Completeness [%] | 99.7 | 99 |
Redundancy | 5.8 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 12% PEG 20000, 0.1 M NA-K-PHOSPHATE PH 6.5 |