4C8F
mouse ZNRF3 ectodomain crystal form IV
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-01-27 |
| Detector | DECTRIS PIXEL |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 109.198, 112.629, 62.220 |
| Unit cell angles | 90.00, 91.01, 90.00 |
Refinement procedure
| Resolution | 41.430 - 2.690 |
| R-factor | 0.23995 |
| Rwork | 0.235 |
| R-free | 0.34053 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.577 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 49.000 |
| High resolution limit [Å] | 2.700 |
| Rmerge | 0.130 |
| Number of reflections | 18914 |
| <I/σ(I)> | 7.8 |
| Completeness [%] | 90.4 |
| Redundancy | 4.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
