4C8C
mouse ZNRF3 ectodomain crystal form III
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-02-22 |
| Detector | PILATUS |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 58.206, 69.617, 75.411 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 46.120 - 2.400 |
| R-factor | 0.23942 |
| Rwork | 0.236 |
| R-free | 0.31980 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.706 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 46.800 |
| High resolution limit [Å] | 2.400 |
| Rmerge | 0.070 |
| Number of reflections | 10823 |
| <I/σ(I)> | 14.4 |
| Completeness [%] | 87.3 |
| Redundancy | 7.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
