4C8A

mouse ZNRF3 ectodomain crystal form II

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I24
Synchrotron site	Diamond
Beamline	I24
Temperature [K]	100
Detector technology	CCD
Collection date	2013-02-22
Detector	ADSC CCD
Spacegroup name	C 1 2 1
Unit cell lengths	71.284, 76.454, 89.331
Unit cell angles	90.00, 93.26, 90.00

Refinement procedure

Resolution	52.150 - 2.700
R-factor	0.22726
Rwork	0.224
R-free	0.29852
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.012
RMSD bond angle	1.518
Refinement software	REFMAC (5.7.0029)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	52.090
High resolution limit [Å]	2.700	2.700
Rmerge	0.060
Number of reflections	13223
<I/σ(I)>	20.6
Completeness [%]	99.5
Redundancy	9.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1