4C86
mouse ZNRF3 ectodomain crystal form I
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-01-27 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 47.296, 57.797, 50.509 |
| Unit cell angles | 90.00, 97.57, 90.00 |
Refinement procedure
| Resolution | 37.870 - 2.000 |
| R-factor | 0.20365 |
| Rwork | 0.200 |
| R-free | 0.27596 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.591 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 37.840 |
| High resolution limit [Å] | 2.000 |
| Rmerge | 0.090 |
| Number of reflections | 16920 |
| <I/σ(I)> | 9.7 |
| Completeness [%] | 91.8 |
| Redundancy | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
