4C85

zebrafish ZNRF3 ectodomain crystal form II

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I24
Synchrotron site	Diamond
Beamline	I24
Temperature [K]	100
Detector technology	PIXEL
Collection date	2013-03-03
Detector	DECTRIS PILATUS 6M
Spacegroup name	P 41 21 2
Unit cell lengths	52.367, 52.367, 204.193
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.640 - 2.500
R-factor	0.22471
Rwork	0.221
R-free	0.30134
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.011
RMSD bond angle	1.464
Refinement software	REFMAC (5.7.0029)

Data quality characteristics

	Overall
Low resolution limit [Å]	46.600
High resolution limit [Å]	2.500
Rmerge	0.090
Number of reflections	10339
<I/σ(I)>	10.1
Completeness [%]	98.0
Redundancy	2.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1