4C84
zebrafish ZNRF3 ectodomain crystal form I
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-05-04 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 35.948, 53.296, 72.459 |
Unit cell angles | 90.00, 102.10, 90.00 |
Refinement procedure
Resolution | 42.630 - 1.600 |
R-factor | 0.22331 |
Rwork | 0.222 |
R-free | 0.25879 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.008 |
RMSD bond angle | 1.199 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 42.590 |
High resolution limit [Å] | 1.600 |
Rmerge | 0.070 |
Number of reflections | 35475 |
<I/σ(I)> | 16.1 |
Completeness [%] | 99.8 |
Redundancy | 11 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |