4C83
Crystal Structure of the IgG2a LPT3 in complex with an 8-sugar inner core analogue of Neisseria meningitidis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Spacegroup name | P 1 |
Unit cell lengths | 62.628, 64.192, 64.403 |
Unit cell angles | 87.51, 89.82, 73.41 |
Refinement procedure
Resolution | 37.900 - 2.690 |
R-factor | 0.22845 |
Rwork | 0.225 |
R-free | 0.29255 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mf2 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.321 |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.790 |
High resolution limit [Å] | 2.690 | 2.690 |
Rmerge | 0.050 | 0.140 |
Number of reflections | 26006 | |
<I/σ(I)> | 10.3 | 3.3 |
Completeness [%] | 97.5 | 98.1 |
Redundancy | 1.96 | 1.95 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |