4C3B
HRSV M2-1, P21 crystal form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-12-16 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 91.853, 141.616, 141.694 |
Unit cell angles | 90.00, 96.14, 90.00 |
Refinement procedure
Resolution | 140.880 - 2.950 |
R-factor | 0.20787 |
Rwork | 0.205 |
R-free | 0.25458 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.523 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 140.880 | 3.010 |
High resolution limit [Å] | 2.950 | 2.950 |
Rmerge | 0.190 | 1.380 |
Number of reflections | 75535 | |
<I/σ(I)> | 14.4 | 2.3 |
Completeness [%] | 99.5 | 98.2 |
Redundancy | 15 | 14.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 10 | 30 % (V/V) PEG 400, 0.1 M CAPS PH 10 |