4C30
Crystal structure of Deinococcus radiodurans UvrD in complex with DNA, form 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 68.489, 89.785, 293.798 |
Unit cell angles | 90.00, 89.97, 90.00 |
Refinement procedure
Resolution | 66.180 - 3.000 |
R-factor | 0.23114 |
Rwork | 0.228 |
R-free | 0.28783 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | DRUVRD FORM1 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.544 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0085) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.200 | 3.160 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.060 | 0.320 |
Number of reflections | 62649 | |
<I/σ(I)> | 6.5 | 1.9 |
Completeness [%] | 89.0 | 86.5 |
Redundancy | 1.5 | 1.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 22% PEG 3350, 0.1 M BIS-TRIS PROPANE PH 7.5, 0.1 M NA-FLUORIDE |