4C2U
Crystal structure of Deinococcus radiodurans UvrD in complex with DNA, Form 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.572, 67.448, 386.040 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.740 - 2.550 |
R-factor | 0.2141 |
Rwork | 0.211 |
R-free | 0.26651 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3pjr |
RMSD bond length | 0.017 |
RMSD bond angle | 1.744 |
Data scaling software | SCALA |
Phasing software | MrBUMP |
Refinement software | REFMAC (5.6.0085) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.400 | 2.690 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.070 | 0.590 |
Number of reflections | 56088 | |
<I/σ(I)> | 20.4 | 3.6 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.3 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 20% PEG 3350, 0.1 M BIS-TRIS PROPANE PH 7.0, 0.2 M NA-NITRATE |