4C18
The structure of the Tsi2 dimer with a disulfide bond
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 113 |
Detector technology | CCD |
Collection date | 2011-07-11 |
Detector | MARRESEARCH |
Spacegroup name | P 1 |
Unit cell lengths | 27.970, 36.300, 37.860 |
Unit cell angles | 107.37, 95.23, 92.11 |
Refinement procedure
Resolution | 34.590 - 1.490 |
R-factor | 0.22445 |
Rwork | 0.223 |
R-free | 0.25886 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3vpv |
RMSD bond length | 0.018 |
RMSD bond angle | 1.812 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.930 | 1.570 |
High resolution limit [Å] | 1.490 | 1.490 |
Rmerge | 0.110 | 0.240 |
Number of reflections | 21050 | |
<I/σ(I)> | 7.3 | 3.7 |
Completeness [%] | 92.0 | 88.6 |
Redundancy | 3.8 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.1M SODIUM CITRATE PH 5.6, 35% T-BUTANOL |