4C0W
The crystal strucuture of native PpAzoR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315r |
Spacegroup name | F 2 2 2 |
Unit cell lengths | 72.299, 95.743, 146.539 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.130 - 1.600 |
R-factor | 0.1541 |
Rwork | 0.153 |
R-free | 0.17930 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.280 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 53.700 |
High resolution limit [Å] | 1.600 |
Rmerge | 0.050 |
Number of reflections | 33249 |
<I/σ(I)> | 13.9 |
Completeness [%] | 99.1 |
Redundancy | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 293 | 4% PEG 400, 2M AMMONIUM SULPHATE, 0.1M HEPES PH 7.0 AT 293K |