4BZG
Crystal structure of galactose mutarotase GalM from Bacillus subtilis in complex with maltose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2012-12-03 |
Detector | MAR scanner 345 mm plate |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 82.461, 84.202, 125.445 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.670 - 2.130 |
R-factor | 0.18504 |
Rwork | 0.183 |
R-free | 0.22671 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3mwx |
RMSD bond length | 0.013 |
RMSD bond angle | 1.567 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.670 | 2.240 |
High resolution limit [Å] | 2.130 | 2.130 |
Rmerge | 0.110 | 0.570 |
Number of reflections | 49195 | |
<I/σ(I)> | 13.2 | 3.4 |
Completeness [%] | 98.5 | 89.8 |
Redundancy | 7 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |