4BYY
Apo GlxR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 95.643, 59.936, 90.880 |
Unit cell angles | 90.00, 110.70, 90.00 |
Refinement procedure
Resolution | 85.010 - 2.480 |
R-factor | 0.21264 |
Rwork | 0.209 |
R-free | 0.28666 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.012 |
RMSD bond angle | 1.673 |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 85.000 |
High resolution limit [Å] | 2.480 |
Rmerge | 0.040 |
Number of reflections | 17204 |
Completeness [%] | 99.7 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |