4BXD
CRYSTAL STRUCTURE OF AMPDH3 FROM PSEUDOMONAS AERUGINOSA IN COMPLEX WITH TETRASACCHARIDE PENTAPEPTIDE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-02-09 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 101.186, 101.186, 162.261 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.300 - 3.100 |
R-factor | 0.2262 |
Rwork | 0.224 |
R-free | 0.27720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | AMPDH3-NATIVE |
RMSD bond length | 0.023 |
RMSD bond angle | 1.899 |
Data scaling software | SCALA |
Phasing software | iMOSFLM |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.300 | 3.270 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.080 | 0.260 |
Number of reflections | 15988 | |
<I/σ(I)> | 21.8 | 7.6 |
Completeness [%] | 100.0 | 100 |
Redundancy | 10.8 | 8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |