4BWD
Human short coiled coil protein
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-12-07 |
Detector | DECTRIS PILATUS |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 70.980, 114.750, 93.270 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.905 - 2.702 |
R-factor | 0.2209 |
Rwork | 0.219 |
R-free | 0.26010 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.008 |
RMSD bond angle | 0.999 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.070 | 0.580 |
Number of reflections | 10743 | |
<I/σ(I)> | 17.3 | 3.7 |
Completeness [%] | 99.5 | 96.4 |
Redundancy | 6.5 | 6.44 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.6 | 0.01 M COBALT CHLORIDE 0.1 M SODIUM ACETATE PH 4.63, 0.7 M 1,6 HEXANEDIOL |