4BVP
Legionella pneumophila NTPDase1 crystal form II (closed) in complex with heptamolybdate and octamolybdate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 100 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 64.564, 85.436, 71.779 |
| Unit cell angles | 90.00, 103.94, 90.00 |
Refinement procedure
| Resolution | 45.340 - 1.490 |
| R-factor | 0.12652 |
| Rwork | 0.126 |
| R-free | 0.16858 |
| Structure solution method | OTHER |
| RMSD bond length | 0.021 |
| RMSD bond angle | 2.577 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 45.300 |
| High resolution limit [Å] | 1.490 |
| Rmerge | 0.060 |
| Number of reflections | 119751 |
| <I/σ(I)> | 18.4 |
| Completeness [%] | 96.5 |
| Redundancy | 6.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 100MM NAMES PH 5.2, 11% PEG3350, 20MM MGCL2 |
