Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4BUW

Crystal structure of human tankyrase 2 in complex with 2-(4-(2-oxo-1, 3-oxazolidin-3-yl)phenyl)-3,4-dihydroquinazolin-4-one

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-4
Synchrotron siteESRF
BeamlineID14-4
Temperature [K]100
Detector technologyCCD
Collection date2012-06-20
DetectorADSC CCD
Spacegroup nameC 2 2 21
Unit cell lengths91.150, 98.030, 118.610
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution49.010 - 1.850
R-factor0.15477
Rwork0.153
R-free0.19246
Structure solution methodOTHER
Starting model (for MR)NONE
RMSD bond length0.012
RMSD bond angle1.571
Data reduction softwareXDS
Data scaling softwareXSCALE
Refinement softwareREFMAC (5.7.0029)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.900
High resolution limit [Å]1.8501.850
Rmerge0.0700.640
Number of reflections45417
<I/σ(I)>16.12.23
Completeness [%]99.696.5
Redundancy4.83.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.52770.2 M LISO4, 0.1 M TRIS HCL, 22% PEG3350, PH 8.5, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 277K

223532

PDB entries from 2024-08-07

PDB statisticsPDBj update infoContact PDBjnumon