4BTJ
TTBK1 in complex with ATP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 125.980, 110.020, 110.550 |
| Unit cell angles | 90.00, 93.85, 90.00 |
Refinement procedure
| Resolution | 21.770 - 2.160 |
| R-factor | 0.1794 |
| Rwork | 0.178 |
| R-free | 0.19680 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.040 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Refinement software | BUSTER (2.11.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 21.770 | 2.220 |
| High resolution limit [Å] | 2.160 | 2.160 |
| Rmerge | 0.070 | 0.520 |
| Number of reflections | 79065 | |
| <I/σ(I)> | 11.3 | 2.1 |
| Completeness [%] | 98.1 | 87.3 |
| Redundancy | 3.4 | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
