4BSP

Crystal structure of R-spondin 1 (Fu1Fu2) - Holmium soak

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-1
Synchrotron site	ESRF
Beamline	ID23-1
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	I 2 2 2
Unit cell lengths	35.630, 64.560, 92.370
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	52.916 - 2.000
R-factor	0.2296
Rwork	0.228
R-free	0.26030
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.006
RMSD bond angle	0.873
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	33.200
High resolution limit [Å]	2.000
Rmerge	0.120
Number of reflections	7500
<I/σ(I)>	11.2
Completeness [%]	99.7
Redundancy	10

Crystallization Conditions

crystal ID	method	pH	temperature	details
1