4BSP
Crystal structure of R-spondin 1 (Fu1Fu2) - Holmium soak
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 35.630, 64.560, 92.370 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 52.916 - 2.000 |
R-factor | 0.2296 |
Rwork | 0.228 |
R-free | 0.26030 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.006 |
RMSD bond angle | 0.873 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 33.200 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.120 |
Number of reflections | 7500 |
<I/σ(I)> | 11.2 |
Completeness [%] | 99.7 |
Redundancy | 10 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |